Development of High Purity, Few-Layer Graphene Synthesis by Electric Arc Discharge Technique

dc.contributor.authorÇotul, Uğur
dc.contributor.authorŞam Parmak, Ebru Devrim
dc.contributor.authorKaykilarli, C.
dc.contributor.authorSaray, O.
dc.contributor.authorColak, O.
dc.contributor.authorUzunsoy, Deniz
dc.date.accessioned2021-03-20T20:13:09Z
dc.date.available2021-03-20T20:13:09Z
dc.date.issued2018
dc.departmentBTÜ, Mühendislik ve Doğa Bilimleri Fakültesi, Metalurji ve Malzeme Mühendisliği Bölümüen_US
dc.description7th International Advances in Applied Physics and Materials Science Congress and Exhibition (APMAS) -- APR 22-26, 2017 -- Fethiye, TURKEYen_US
dc.descriptionKAYKILARLI, Cantekin/0000-0002-2380-3258en_US
dc.description.abstractIn this study, high purity graphene nanoflakes (GNF) were synthesized by electric arc discharge technique. The arc discharge method is more advantageous than other graphene synthesis methods for producing cheap and good-quality graphene with minimum defects and not including dangerous chemicals. Because of this advantages, the arc discharge method is one step ahead of all graphene synthesis methods. In order to synthesize GNF, a DC electric arc discharge reactor was designed by our team. Electric arc discharge method based on a principle that provides a constant current between two high purity graphite electrodes to vaporize. After the arc discharge, nanoparticles accumulate on the inner surface of the reactor. The voltage stabilizer DC power source is used to create a current in the environment and the discharge usually occurs in a range 20-60 V. This current can be adjusted depending on the diameter of electrodes, the distance between electrodes and arc current varies between 100 and 150 A. Different characterization techniques such as the Raman spectroscopy, scanning electron microscope and transmission electron microscope were used to characterize the graphene layers synthesized by the arc discharge method. The L-D / L-G ratio was calculated as 0.66 while the L-G / L-2D was determined as 1.31. These values show that the purity of the synthesized graphene is compatible to that of commercially supplied graphene. Besides, the synthesized graphene has fewer layer than commercially supplied one. Transmission electron microscope observations confirmed the typical wrinkled feature of graphene.en_US
dc.description.sponsorshipTUBITAKTurkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK) [215M031]en_US
dc.description.sponsorshipThis work has been supported by TUBITAK Project Number of 215M031.en_US
dc.identifier.doi10.12693/APhysPolA.134.289en_US
dc.identifier.endpage291en_US
dc.identifier.issn0587-4246
dc.identifier.issn1898-794X
dc.identifier.issue1en_US
dc.identifier.scopusqualityQ4en_US
dc.identifier.startpage289en_US
dc.identifier.urihttp://doi.org/10.12693/APhysPolA.134.289
dc.identifier.urihttps://hdl.handle.net/20.500.12885/803
dc.identifier.volume134en_US
dc.identifier.wosWOS:000451281600077en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorÇotul, Uğur
dc.language.isoenen_US
dc.publisherPolish Acad Sciences Inst Physicsen_US
dc.relation.ispartofActa Physica Polonica Aen_US
dc.relation.publicationcategoryKonferans Öğesi - Uluslararası - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectgraphiteen_US
dc.subjectgrapheneen_US
dc.subjectelectric arc-dischargeen_US
dc.subjectRaman spectroscopyen_US
dc.titleDevelopment of High Purity, Few-Layer Graphene Synthesis by Electric Arc Discharge Techniqueen_US
dc.typeConference Objecten_US

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