Determination of insecticides in honey samples collected from Gümüşhane-Turkiye; Box-Behnken design evaluation of experimental parameters

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dc.contributor.authorErçağ, Erol
dc.contributor.authorYalçın, Berrin Saygı
dc.contributor.authorŞahin, Murat
dc.contributor.authorYücesoy, Fehime Jülide Hızal
dc.date.accessioned2026-02-08T15:05:25Z
dc.date.available2026-02-08T15:05:25Z
dc.date.issued2025
dc.departmentBursa Teknik Üniversitesi
dc.description.abstractThis study deals with the investigation of cyfluthrin, cypermethrin, deltamethrin, and malathion residues in local honey samples from Gümüşhane, Turkey. The determination was performed with GC/MS-MS method with HP-5MS column under certain conditions: 120 ? oven temperature, 250 ? injection temperature, 121.9 kPa pressure and 1.2-1.8 mL/min flow rates. The samples were picked from eighteen stations of Gümüşhane. Standard addition method was employed in chromatographic determination. No pesticide detected in samples of fifteen stations, nevertheless, subjected pesticides were determined in samples collected from other three stations. The residue levels varied from 0.18 mg/kg to 9.50 mg/kg at 1.5 mL/min flow rate. The results were also evaluated with Box-Behnken Design (BBD) optimization. Multivariate experimental design (flow rate and station, pesticide type) was employed for constructing quadratic models. Regression analysis showed that the experimental results and the predictive values yielded by model are quite close to each other with determination coefficient (R2) of 0.985.
dc.description.abstractThis study deals with the investigation of cyfluthrin, cypermethrin, deltamethrin, and malathion residues in local honey samples from Gümüşhane, Turkey. The determination was performed with GC/MS-MS method with HP-5MS column under certain conditions: 120 ? oven temperature, 250 ? injection temperature, 121.9 kPa pressure and 1.2-1.8 mL/min flow rates. The samples were picked from eighteen stations of Gümüşhane. Standard addition method was employed in chromatographic determination. No pesticide detected in samples of fifteen stations, nevertheless, subjected pesticides were determined in samples collected from other three stations. The residue levels varied from 0.18 mg/kg to 9.50 mg/kg at 1.5 mL/min flow rate. The results were also evaluated with Box-Behnken Design (BBD) optimization. Multivariate experimental design (flow rate and station, pesticide type) was employed for constructing quadratic models. Regression analysis showed that the experimental results and the predictive values yielded by model are quite close to each other with determination coefficient (R2) of 0.985.
dc.identifier.doi10.61112/jiens.1567692
dc.identifier.endpage186
dc.identifier.issn2791-7630
dc.identifier.issue1
dc.identifier.startpage176
dc.identifier.urihttps://doi.org/10.61112/jiens.1567692
dc.identifier.urihttps://hdl.handle.net/20.500.12885/4666
dc.identifier.volume5
dc.language.isoen
dc.publisherİdris Karagöz
dc.relation.ispartofYenilikçi Mühendislik ve Doğa Bilimleri
dc.relation.ispartofJournal of Innovative Engineering and Natural Science
dc.relation.publicationcategoryMakale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.snmzKA_DergiPark_20260207
dc.subjectEnvironmental and Sustainable Processes
dc.subjectÇevresel ve Sürdürülebilir Süreçler [EN] Food Engineering
dc.subjectGıda Mühendisliği
dc.titleDetermination of insecticides in honey samples collected from Gümüşhane-Turkiye; Box-Behnken design evaluation of experimental parameters
dc.title.alternativeDetermination of insecticides in honey samples collected from Gümüşhane-Turkiye; Box-Behnken design evaluation of experimental parameters
dc.typeArticle

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