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Öğe Biodegradable Nanocomposite Filament Based on PLA/PCL/CNCs for FDM 3D Printing: Production, Characterization and Printability(Wiley, 2025) Ilhan, Recep; Gumus, Omer Yunus; Lekesiz, HuseyinAdditive manufacturing (AM) is a widening technique for the processing of polymers that is not only used by personal users but also by some industries. The development of biodegradable and bio-based composites for AM attracts great interest with respect to various aspects such as environmental issues, user health, and biomedical applications. Polylactic acid (PLA) is a good candidate for bio-based materials. However, its brittleness needs to be improved. In this study, PLA-based filaments with improved toughness by adding polycaprolactone (PCL) (10% and 20% by weight) and cellulose nanocrystals (CNCs) (5% by weight) were produced for the fused deposition modeling (FDM) technique. The physical, thermal, morphological, and mechanical properties of the produced filaments were comprehensively characterized. All filament diameters were found to be within the suitable range for FDM applications (1.75 +/- 0.05 mm). TGA analyses showed that the filaments could maintain their thermal stability up to approximately 256 degrees C and that the CNCs enhanced their thermal stability. The addition of PCL and CNCs did not cause significant changes in T g and T m of the neat PLA (T g = 58.14 degrees C and T m = 175.93 degrees C). The tensile test results indicated that the PCL and CNCs reinforcement increased the elongation at break from 6.76% to 40.25% and the toughness from 2.94 to 14.48 MJ/m3. In the last part, the three-dimensional (3D) printability was demonstrated by producing auxetic sheets with optimized printing parameters based on MFI, TGA, and DSC data, and good dimensional stability was obtained.Öğe Characterizing the Mechanical Performance of a Bare-Metal Stent with an Auxetic Cell Geometry(Mdpi, 2022) Bhullar, Sukhwinder K.; Lekesiz, Huseyin; Karaca, Ahmet Abdullah; Cho, Yonghyun; Willerth, Stephanie Michelle; Jun, Martin B. G.This study develops and characterizes the distinctive mechanical features of a stainless-steel metal stent with a tailored structure. A high-precision femtosecond laser was used to micromachine a stent with re-entrant hexagonal (auxetic) cell geometry. We then characterized its mechanical behavior under various mechanical loadings using in vitro experiments and through finite element analysis. The stent properties, such as the higher capability of the stent to bear upon bending, exceptional advantage at elevated levels of twisting angles, and proper buckling, all ensured a preserved opening to maintain the blood flow. The outcomes of this preliminary study present a potential design for a stent with improved physiologically relevant mechanical conditions such as longitudinal contraction, radial strength, and migration of the stent.Öğe EXPERIMENTAL AND NUMERICAL INVESTIGATION OF SHORT-TERM BIO-DEGRADATION BEHAVIOR OF 3D PRINTED PLA(Amer Soc Mechanical Engineers, 2022) Ilhan, Recep; Senaysoy, Safa; Lekesiz, HuseyinThere has been an increasing interest for biodegradable polymers in recent years because they can be formed as scaffolds and safely removed from the body without the need for any surgical operation, and contribute to the healing process. However, the main problem in polymer-based biodegradable materials is the inability to obtain tunable biodegradation behavior to match healing, which limits the clinical feasibility of these biomaterials. In this study, it is aimed to model biodegradation behavior from short term experimental data in an effort to reduce time required for determination of bio-degradation parameters. Thus, the degradation behavior can be determined and controlled at a lower cost. In this context, the biodegradation behavior of poly-lactic acid (PLA) polymer which is widely used in biomedical applications, was investigated experimentally and numerically on different days related to fracture bone healing times (5-12 weeks). First, 4.5 mm x 4.5 mm x 4.5 mm cubes were printed using the fused deposition modelling (FDM). Then, printed samples were exposed to degradation in the incubator by immersion in phosphate buffered saline (PBS) solution at 37 degrees C at physiological conditions for different time periods (0, 15, 30, 61 and 90 days). Throughout degradation, water absorption, weight loss, mechanical properties and morphological changes were investigated. Water absorption increases up to 13% within 61 days and then decreases to 10% within 90 days. On the other hand, samples gain 1% weight for the first 15 days and following, start losing weight around 0.3% percent at the end of 90 days. This clearly indicates that degradation occurs and water replaces the degraded material. There are fluctuations in the stiffness values that decrease on the 15 and 61 days but they increase on the 30th and 90th days. The increases in stiffness can be attributed to the compressive resistance of the trapped water content. Microscopic investigation clearly verifies the water content that the colors of the samples (opacity increase) changed while no significant change in its size occurred at different degradation days. Experimental results indicate a degradation and mechanical behavior variation throughout the process while dimensional stability during the 90 day degradation period. Numerical model predicts the stiffness values reasonably well within 15 and 30 days of degradation, but differences for 61 and 90 days. This difference possibly stems from the fact that the numerical model does not include any water inclusion disturbance.Öğe EXPERIMENTAL AND NUMERICAL INVESTIGATION OF SHORT-TERM BIODEGRADATION BEHAVIOR OF 3D PRINTED PLA(American Society of Mechanical Engineers, 2022) Ilhan, Recep; Senaysoy, Safa; Lekesiz, HuseyinThere has been an increasing interest for biodegradable polymers in recent years because they can be formed as scaffolds and safely removed from the body without the need for any surgical operation, and contribute to the healing process. However, the main problem in polymer-based biodegradable materials is the inability to obtain tunable biodegradation behavior to match healing, which limits the clinical feasibility of these biomaterials. In this study, it is aimed to model biodegradation behavior from short term experimental data in an effort to reduce time required for determination of bio-degradation parameters. Thus, the degradation behavior can be determined and controlled at a lower cost. In this context, the biodegradation behavior of poly-lactic acid (PLA) polymer which is widely used in biomedical applications, was investigated experimentally and numerically on different days related to fracture bone healing times (5-12 weeks). First, 4.5 mm x 4.5 mm x 4.5 mm cubes were printed using the fused deposition modelling (FDM). Then, printed samples were exposed to degradation in the incubator by immersion in phosphate buffered saline (PBS) solution at 37 °C at physiological conditions for different time periods (0, 15, 30, 61 and 90 days). Throughout degradation, water absorption, weight loss, mechanical properties and morphological changes were investigated. Water absorption increases up to 13% within 61 days and then decreases to 10% within 90 days. On the other hand, samples gain 1% weight for the first 15 days and following, start losing weight around 0.3% percent at the end of 90 days. This clearly indicates that degradation occurs and water replaces the degraded material. There are fluctuations in the stiffness values that decrease on the 15 and 61 days but they increase on the 30th and 90th days. The increases in stiffness can be attributed to the compressive resistance of the trapped water content. Microscopic investigation clearly verifies the water content that the colors of the samples (opacity increase) changed while no significant change in its size occurred at different degradation days. Experimental results indicate a degradation and mechanical behavior variation throughout the process while dimensional stability during the 90 day degradation period. Numerical model predicts the stiffness values reasonably well within 15 and 30 days of degradation, but differences for 61 and 90 days. This difference possibly stems from the fact that the numerical model does not include any water inclusion disturbance. © © 2022 by ASME.Öğe Innovative reinforcement method for metal foam cell wall using CNTs(Iop Publishing Ltd, 2024) Cilsal, Onur Ozan; Lekesiz, Huseyin; Cakir, M. CemalCarbon nanotubes (CNTs) and their composites are gaining popularity due to their exceptional strength qualities. It is well known that adding CNTs to metal foam composites boosts compressive strength. On the other hand CNT addition is still a costly process due to high cost of the CNTs. This study presents a novel and cost-effective solution by selectively adding CNTs to the structurally weakest regions of aluminum foam materials produced via powder metallurgy, employing a newly developed focused multi-step additive method. The cell borders of aluminum foam are strengthened with multiple spherical layers of CNTs, using a transfer method by initially coating the space holders used at the foaming process. The strength increase effect of this CNT addition method was compared with the widely known aluminum foam production parameters via a 4-parameter design of experiment (DOE) study. Compressive strength values of the samples were evaluated using a constant speed compression test acc. to ISO13314. The compacting pressure, CNT concentration, sintering temperature, and sintering period were chosen as DOE parameters, and 78% of the interactions effecting on final compressive strength could be explained with the model. As a result, it was established that, compared to the other parameters, sintering duration had the highest influence on compressive strength. But besides It has also been shown that adding 0.53% CNT by weight only to the cell border regions increases overall strength by 9%. This weight-strength increase ratio is compared with similar studies in the literature and found to be providing a production cost advantage due to the lower amount of CNT addition requirement for the comparable weight relative strength increase. Focused strength increase method has potential to enable controlled failure of foam materials by selectively strengthening strength critical areas of a component.Öğe Mechanical deviation in 3D-Printed PLA bone scaffolds during biodegradation(Elsevier Ltd, 2024) Senaysoy, Safa; İLhan, Recep; Lekesiz, HuseyinLarge or carcinogenic bone defects may require a challenging bone tissue scaffold design ensuring a proper mechanobiological setting. Porosity and biodegradation rate are the key parameters controlling the bone-remodeling process. PLA presents a great potential for geometrically flexible 3-D scaffold design. This study aims to investigate the mechanical variation throughout the biodegradation process for lattice-type PLA scaffolds using both experimental observations and simulations. Three different unit-cell geometries are used for creating the scaffolds: basic cube (BC), body-centered structure (BCS), and body-centered cube (BCC). Three different porosity ratios, 50 %, 62.5 %, and 75 %, are assigned to all three structures by altering their strut dimensions. 3-D printed scaffolds are soaked in PBS solution at 37 °C for 15, 30, 60, 90, and 120 days both unloaded and under dead load. Water absorption, weight loss, and compression stiffness are measured to characterize the first-stage degradation and investigate the possible influences of these parameters on the whole biodegradation process. The strength reduction stage of biodegradation is simulated by solving pseudo-first-order kinetics-based molecular weight change equation using FEA with equisized cubic (voxel-like) elements. For the first stage, mechanical load does not have a statistically significant effect on biodegradation. BCC with 62.5 % porosity shows a maximum water absorption rate of around 25 % by the 60th day which brings an advantage in creating an aquatic environment for cell growth. Results indicate a significant water deposition inside almost all scaffolds and water content is determined to be the main reason for the retained or increased compression stiffness. A distinguishable stiffness increase in the initial degradation process occurs for 75 % porous BC and 50 % porous BCC scaffolds. Following the quasi-stable stage of biodegradation, almost all scaffolds lost their rigidity by around 44–48 % within 120 days based on numerical results. Therefore, initial stiffness increase in the quasi-stable stage of biodegradation can be advantageous and BCC geometry with a porosity between 50% and 62 % is the optimum solution for the whole biodegradation process. © 2024 Elsevier LtdÖğe Minimization of release bearing load loss in a clutch system for high-speed rotations using the differential evolution algorithm(Walter De Gruyter Gmbh, 2022) Karaduman, Alper; Lekesiz, Huseyin; Yildiz, Ali RizaDiaphragm spring is a critical part of a clutch system because it affects the release bearing load characteristics directly and that determines the quality of disengagement. Bearing load provides required clamping for coupling however it may vary significantly during the engagement/disengagement process. A significant drop in bearing load may be experienced especially for high engine velocities for certain bearing displacement due to centrifugal forces occurring on the fingertips of diaphragm springs. The falling in release bearing load is undesirable for comfortable driving and clutch performance. This problem has not been addressed clearly in technical literature. In this study, the diaphragm spring for a C-segment passenger car is optimized using a differential evolutionary algorithm, and an optimized diaphragm was manufactured for testing. The load-bearing characteristics of the optimized diaphragm were compared with those of the currently available diaphragm spring. Loss of bearing load occurring in high-speed rotations was significantly reduced for the optimized diaphragm. Parameters influencing the performance were identified using parameter influence analysis, and a robust disengagement behavior was actualized using the optimization process.Öğe The Development of an Innovative Occupational Passive Upper Extremity Exoskeleton and an Investigation of Its Effects on Muscles(Mdpi, 2023) Ocal, Ahmet Emre; Lekesiz, Huseyin; Cetin, Sevda TelliWork-related musculoskeletal disorders are one of the main problems reducing the life quality of workers. Occupational exoskeletons are one of the most promising solutions for solving this issue. In this study, an innovative and passive upper-extremity exoskeleton design was presented and tested by measuring ten different muscle activities for two tasks: Task 1, for over-the-head tool handling, and Task 2, for completely stretched forearm tool handling. The special optimized switch mechanism design allowed for free motion when it was not active, which provided design advantages in comparison to the currently available designs. The muscle activity levels were measured via EMG for both tasks and the results were compared and evaluated with and without the exoskeleton on the human body. It was shown that the muscle activity for Task 1 was reduced by 55% for the middle deltoid, 37% for the posterior deltoid, and 27% for the anterior deltoid muscles, in comparison to no exoskeleton for Task 1. For Task 2, the muscle activity was reduced by 48% for the middle deltoid, 20% for the posterior deltoid, and 38% for the anterior deltoid. The exoskeleton presented in this study is an efficient design that significantly increases shoulder comfort, especially in working conditions, without bringing an additional metabolic cost for the secondary muscles.
